The Laboratory: Equipment and Safety Rules
In your school's Physical Science class, you need to measure about 25 mL of water for an experiment. On the table there is a beaker, a graduated cylinder, and an Erlenmeyer flask. Which one do you choose? Choosing the right instrument, and working safely, is the first skill of anyone who does science.
Measuring Instruments
Match each piece of lab equipment with its use: a) Measuring cylinder b) Thermometer c) Balance 1) Measuring the temperature of water. 2) Measuring a volume of liquid…
Match each piece of lab equipment with its use:
- a) Measuring cylinder
- b) Thermometer
- c) Balance
1) Measuring the temperature of water.
2) Measuring a volume of liquid fairly accurately.
3) Measuring the mass of a solid.
You need to measure exactly $25\ \text{mL}$ of water for an experiment. The three containers are shown in the figure: Which piece of apparatus would you use: a beaker, a…
You need to measure exactly $25\ \text{mL}$ of water for an experiment. The three containers are shown in the figure:
Which piece of apparatus would you use: a beaker, a measuring cylinder or a conical flask? Justify your choice.
The conical flask is wide at the base and narrow at the neck, as shown in the figure. Explain what advantage this shape has when swirling a mixture.
The conical flask is wide at the base and narrow at the neck, as shown in the figure.
Explain what advantage this shape has when swirling a mixture.
Measuring Well: Precision and Setup
An instrument is more precise when its scale has smaller divisions: the error you make when reading it is smaller. A graduated cylinder with marks every $2\ \text{mL}$ is more precise than a beaker with marks every $50\ \text{mL}$.
With the thermometer, the setup also matters. If you are heating water, the bulb must not touch the bottom of the beaker: the bottom is in contact with the heat source and is hotter than the water, so the reading would come out higher than the real temperature of the water. The thermometer is held by a stand, submerged in the liquid without touching the glass.
Using the balance, you measure an empty beaker: $50\ \text{g}$. Then you fill it with water and it reads $125\ \text{g}$. a) What mass of water have you poured in? b)…
Using the balance, you measure an empty beaker: $50\ \text{g}$. Then you fill it with water and it reads $125\ \text{g}$.
- a) What mass of water have you poured in?
- b) Explain why it is necessary to measure the empty beaker first.
A measuring cylinder contains $30\ \text{mL}$ of water and you add $45\ \text{mL}$ more, measured with another measuring cylinder. a) What total volume is there now? b)…
A measuring cylinder contains $30\ \text{mL}$ of water and you add $45\ \text{mL}$ more, measured with another measuring cylinder.
- a) What total volume is there now?
- b) Explain why a measuring cylinder is used to measure volumes rather than a beaker, even if the beaker has some graduations.
You need to mix water and salt by swirling without splashing. The two containers are shown in the figure: Which container would you choose: a wide-mouthed beaker or a…
You need to mix water and salt by swirling without splashing. The two containers are shown in the figure:
Which container would you choose: a wide-mouthed beaker or a conical flask? Explain your choice by referring to the shape of each one.
When measuring the temperature of heated water, the thermometer must not touch the bottom of the beaker. Observe the setup in the figure: a) Explain why. b) If the…
When measuring the temperature of heated water, the thermometer must not touch the bottom of the beaker. Observe the setup in the figure:
- a) Explain why.
- b) If the bottom is hotter than the water, would the reading be higher or lower than the actual temperature?
You have a measuring cylinder with graduations every $2\ \text{mL}$ and a beaker with graduations every $50\ \text{mL}$, as shown in the figure. You need to measure…
You have a measuring cylinder with graduations every $2\ \text{mL}$ and a beaker with graduations every $50\ \text{mL}$, as shown in the figure.
You need to measure $36\ \text{mL}$ of water.
- a) Which piece of apparatus do you choose?
- b) Justify your choice by considering the error you would make with each one.
- c) Using this example, explain what it means for an instrument to be "more precise".
Safety Rules
Every rule has its reason. You do not eat or drink because containers and the table can have invisible traces of dangerous substances. You do not pour leftovers back because it would contaminate the whole bottle. You label because an unlabeled liquid cannot be identified and someone could use it by mistake. You wash and clean up so the next group does not find residues and to avoid accidents.
The Burner
The burner is used for heating. Before lighting it: hair tied back, papers and flammable products far away, and the table cleared. It is never left lit without someone using it, and you do not bring your face close to the flame.
Responsible Use of Resources
The laboratory belongs to everyone and its resources cost money: the reagents, the water, the gas or electricity, and the glassware. Taking care of them is also a safety rule and a way of respecting the environment.
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Reagents: take only the amount the activity calls for. What is left over does not go back into the bottle, so taking too much is waste. Waste is not poured down the sink without asking the teacher.
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Water: do not leave the faucet running while you work or while you wash.
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Gas and electricity: turn off the burner, hot plates, and equipment when you finish. In a country with blackouts and high electricity bills, every kWh counts.
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Equipment: use each instrument for what it is meant for (do not heat a graduated cylinder) and handle it carefully. Broken equipment is replaced with everyone's money.
What is the Bunsen burner used for in the laboratory? Write down two safety rules that must always be followed when using it.
What is the Bunsen burner used for in the laboratory? Write down two safety rules that must always be followed when using it.
Before entering the laboratory, the teacher requires everyone to put on a lab coat and, for some practicals, safety goggles as well. Explain what each protects against.
Before entering the laboratory, the teacher requires everyone to put on a lab coat and, for some practicals, safety goggles as well. Explain what each protects against.
In the laboratory, it is forbidden to taste any substance, even if it looks like water. a) If you need to smell a chemical, how is it done safely? b) Why do you think…
In the laboratory, it is forbidden to taste any substance, even if it looks like water.
- a) If you need to smell a chemical, how is it done safely?
- b) Why do you think this rule exists?
At the next desk, Pablo is dipping a cookie into a beaker of water while his lab partner, who has long loose hair, leans over a lit Bunsen burner. Point out the two…
At the next desk, Pablo is dipping a cookie into a beaker of water while his lab partner, who has long loose hair, leans over a lit Bunsen burner. Point out the two safety mistakes and write down the rule that corrects each one.
Observe this laboratory scene: Carla is working with loose hair, she has left her sandwich on the bench, the Bunsen burner is lit while unattended, a classmate tastes a…
Observe this laboratory scene: Carla is working with loose hair, she has left her sandwich on the bench, the Bunsen burner is lit while unattended, a classmate tastes a liquid "because it looks like lemonade", and there are sheets of paper right next to the flame. Find the five safety mistakes and write down the rule that corrects each one.
Explain the reason for each of these laboratory rules: a) Unused chemicals are never returned to their original container. b) Every container holding a substance must be…
Explain the reason for each of these laboratory rules:
- a) Unused chemicals are never returned to their original container.
- b) Every container holding a substance must be labelled.
- c) At the end of the practical, equipment is washed and the work bench is cleared.
Before starting a practical involving a Bunsen burner, you must prepare the work area. Make a list of at least four things you should do or remove before lighting the…
Before starting a practical involving a Bunsen burner, you must prepare the work area. Make a list of at least four things you should do or remove before lighting the flame, and justify each one in a sentence.
Hazard Pictograms
Chemical products carry risk symbols on the label: a diamond with a red border and a drawing that warns of the danger at a glance. They are always read together with the full label.
On the label of some alcohol you see a pictogram with a flame, and on another chemical, a skull and crossbones. Observe the two pictograms: a) What hazard does each…
On the label of some alcohol you see a pictogram with a flame, and on another chemical, a skull and crossbones. Observe the two pictograms:
- a) What hazard does each pictogram indicate?
- b) What precaution would you take with each chemical?
You are going to use alcohol, whose label bears the flame pictogram (flammable), and on the adjacent bench there is a lit Bunsen burner. Write down two specific…
You are going to use alcohol, whose label bears the flame pictogram (flammable), and on the adjacent bench there is a lit Bunsen burner. Write down two specific precautions you must take and explain what the hazard is.
You need to use a chemical with the skull pictogram (toxic) and, in another practical, alcohol with the flame pictogram (flammable). a) Write down two specific safety…
You need to use a chemical with the skull pictogram (toxic) and, in another practical, alcohol with the flame pictogram (flammable).
- a) Write down two specific safety measures for each chemical.
- b) Explain why the measures are different in each case.
You must heat $50\ \text{mL}$ of salty water to $40\ ^\circ\text{C}$ and measure the temperature while it heats up. Write down the complete procedure: the required…
You must heat $50\ \text{mL}$ of salty water to $40\ ^\circ\text{C}$ and measure the temperature while it heats up. Write down the complete procedure: the required equipment, the steps in order, and the safety rules you apply at each stage, justifying at least two of them.
What to Do If Something Goes Wrong
You drop a test tube on the floor and it breaks. State two things you should do immediately and one thing you must never do.
You drop a test tube on the floor and it breaks. State two things you should do immediately and one thing you must never do.
A few drops of an irritant chemical splash onto your lab partner's hand. Write down two actions she should take immediately and one thing she must not do.
A few drops of an irritant chemical splash onto your lab partner's hand. Write down two actions she should take immediately and one thing she must not do.
You are going to heat $100\ \text{mL}$ of water and want to record its temperature every minute. a) Make a list of the equipment you need (at least four items). b)…
You are going to heat $100\ \text{mL}$ of water and want to record its temperature every minute.
- a) Make a list of the equipment you need (at least four items).
- b) Write, in order, the steps you will follow.
A student spills a small amount of dilute acid on their hand. a) Write down the correct actions in order. b) Explain why home remedies such as toothpaste or oil should…
A student spills a small amount of dilute acid on their hand.
- a) Write down the correct actions in order.
- b) Explain why home remedies such as toothpaste or oil should not be applied.
- c) State what information you must give to the teacher.
A test tube falls to the floor, breaks, and the liquid spills across the floor. a) Describe the complete, step-by-step protocol to act safely: reporting the incident,…
A test tube falls to the floor, breaks, and the liquid spills across the floor.
- a) Describe the complete, step-by-step protocol to act safely: reporting the incident, cordoning off the area, what to use to sweep up the glass, and how to deal with the liquid.
- b) Justify why glass must not be picked up with your hands.
Back to the start: to measure the 25 mL of water precisely, you choose the graduated cylinder; the beaker and the Erlenmeyer flask only have approximate marks.